Actually, Norma ballistic lab can reproduce it almost at will (if not at will). Since the Krupp Commission most manufacturers take their findings in count. But it is also documented from when they developped the "slower" burning powders after WWI - DuPont, ICI, Nobel all experienced it. P.O. Ackley is one who was almost successful in reproducing it at will and in the '50's, he then joined with Norma to do more experiments, each on their sides, comparing their results, which later brang their conclusions.