Thought I would update you on my endeavours. Tried water again. A little better luck no popcorn but shot all had tails on it. Nothing nice like what joehunt is able to get.
So I tried Fabric Softner. Got the cheapest I could get at Canadian Tire. I tried it first using a 6 3/4 deep x 10 x 3 3/4 inch wide 9mm ammo tin. No luck lots of tails and out of round. Figured it was not deep enough to cool before hitting bottom. So then I tried a bigger ammo tin. 8 1/4 x 12 x 7. Holds 800 5.56 rounds. I put in almost 12 litres of softner. Drop to liquid was 3/4 inch. Much better success. Shot was much rounder. I do have some with short tails and others that look like rat poop. So not perfect but very useable IMO. Had to quit after about an hour as liquid was getting too hot.
I will try again soon. I do have a larger container that will hold about 5 gallons and may splurge and go that way once I am convinced this will work. I will also try to reduce drop distance.
Any pointers on why shot may not be totally round, how to get rid of short tails and rat poop?
Thanks again. I guess I am slowly making progress.